By Allen J Bard
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Additional resources for Electrogenerated chemiluminescence
Frank and Park  provide general information on the experimental procedures about electrochemistry in a dry box. However, for vigorous ECL studies, vacuum systems probably offer the best compromise between convenience, flexibility, and effectiveness in handling materials. Deoxygenation is rigorously accomplished by three or four freeze–pump–thaw cycles, and the cell can be protectively filled with argon or helium afterward. This procedure results in negligible loss of solvents for nonvolatile DMF and benzonitrile, but care is needed for volatile solvents such as acetonitrile and tetrahydrofuran.
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Was involved in double-layer charging, so no light was generated at the counter electrode. Solutions were prepared by transferring 5 mL of the solvent under vacuum at Ϫ30°C into the degassing arm containing the supporting electrolyte and the compound, which had been predried for 12 h at Ͻ10Ϫ5 torr. After two freeze–pump–thaw cycles the solution was transferred directly to the sample compartment. In constructing the cell, sufficient care was Copyright © 2004 by Marcel Dekker, Inc. Experimental Techniques of ECL Figure 3 31 Variable temperature ECL and electrochemical cell.
Electrogenerated chemiluminescence by Allen J Bard