By William L. Luyben
Chapter 1 advent (pages 1–10):
Chapter 2 part Equilibrium (pages 11–43):
Chapter three Steady?State layout in Aspen Plus (pages 45–95):
Chapter four Dynamics and keep watch over in Aspen Dynamics (pages 97–145):
Chapter five Pressure?Swing Azeotropic Distillation (pages 149–164):
Chapter 6 strain Swing with warmth Integration (pages 165–197):
Chapter 7 Heterogeneous Binary Azeotropes (pages 199–215):
Chapter eight Isopropanol–Water (Cyclohexane because the Entrainer) (pages 219–244):
Chapter nine Acetic Acid–Water (Isobutyl Acetate because the Entrainer) (pages 245–295):
Chapter 10 Isopropanol–Water (Dimethyl Sulfoxide because the Entrainer) (pages 299–325):
Chapter eleven Extractive Distillation of the Acetone–Methanol process (pages 327–367):
Chapter 12 Maximum?Boiling Azeotropes (pages 369–383):
Chapter thirteen Batch Distillation of Azeotropes (pages 387–428):
Chapter 14 Hybrid Distillation–Pervaporation platforms (pages 429–450):
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Additional resources for Design and Control of Distillation Systems for Separating Azeotropes
9. Select the Mole checkbox under the Fraction basis column in the middle of the window. With the bookkeeping issues out of the way, we can select the chemical components by clicking Components on the left of the Data Browser window. 10. Clicking the Find buttons near the bottom of the window opens another window. 11. A list of components is opened at the bottom of the window. Click ISOPROPYL ALCOHOL and click the Add button at the bottom of the window. Repeat for Water and dimethyl sulfoxide and click Close.
9. 10 will be displayed (the dashed line near the acetone apex of the triangle). Remember that the volatility between acetone and methanol is unity in the binary system when we are at the azeotrope (shown on the ordinate in Fig. 248C). 10 (where the concentration of methanol goes to zero). The location where this isovolatility curve intercepts the acetone – DMSO edge of the triangle is important in determining if DMSO is an effective entrainer. Usually, the closer the intersection point is to the original component corner, the less entrainer is required, which means lower operating and capital costs.
21 Enter more data. 22 Name of the second dataset. 23 Input second Txy dataset near azeotropic point. options of the objective function, the maximum iterations, and the step size can be specified. We go with the default selection of using the Maximum-Likelihood method. 29. 30 to start the regression run. 31 shows that the data regression run is complete with six iterations. 24 Specify the regression case. 25 Name the regression case. To know the resulting binary parameters, the folder selection as: Properties !
Design and Control of Distillation Systems for Separating Azeotropes by William L. Luyben